Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylene-urea oligomers (method B)

This European Standard specifies methods for the determination of isobutylidenediurea (IBDU), crotonylidenediurea (CDU) (method A) and methylene-urea oligomers (MU) (method B) in fertilizers using high-performance liquid chromatography (HPLC). The method is applicable to all fertilizers which do not contain interfering organic compounds.

Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B)

Diese Europäische Norm legt Verfahren für die Bestimmung von Isobutylidendiharnstoff (IBDU), Crotony-lidendiharnstoff (CDU) (Verfahren A) und Methylenharnstoff-Oligomere (MU) (Verfahren B) in Düngemitteln mit Hochleistungs-Flüssigchromatographie (HPLC) fest.
Das Verfahren gilt für alle Düngemittel, die keine störenden organischen Verbindungen enthalten.

Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylene-urée (méthode B)

La présente Norme européenne spécifie les méthodes de dosage de l’isobutylidène diurée (IBDU), de la crotonylidène diurée (CDU) (méthode A) et des oligomères de méthylène-urée (MU) (méthode B) dans les engrais par chromatographie liquide haute performance (HPLC).
La méthode est applicable à tous les engrais qui ne contiennent pas de composés organiques interférents.

Gnojila - Določevanje kondenzatov sečnine s tekočinsko kromatografijo visoke ločljivosti (HPLC) - Izobutilidendiurea in krotonilidendiurea (metoda A) in oligomeri metilenuree (metoda B)

Ta evropski standard določa metode za določevanje izobutilidendiura(IBDU), krotonilidendiurea(CDU) (metoda A) ter oligomeri metilenuree (MU) (metoda B) v gnojilih s tekočinsko kromatografijo visoke ločljivosti (HPLC). Metoda se uporablja za vsa gnojila, ki ne vsebujejo motečih organskih spojin.

General Information

Status
Withdrawn
Public Enquiry End Date
19-Dec-2009
Publication Date
14-Sep-2010
Withdrawal Date
09-May-2024
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
26-Apr-2024
Due Date
19-May-2024
Completion Date
10-May-2024

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Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B)Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylene-urée (méthode B)Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylene-urea oligomers (method B)65.080GnojilaFertilizersICS:Ta slovenski standard je istoveten z:EN 15705:2010SIST EN 15705:2010en,fr,de01-oktober-2010SIST EN 15705:2010SLOVENSKI
STANDARDSIST-TS CEN/TS 15705:20091DGRPHãþD



SIST EN 15705:2010



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15705
March 2010 ICS 65.080 Supersedes CEN/TS 15705:2009English Version
Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylen-urea oligomers (method B)
Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylène-urée (méthode B)
Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B) This European Standard was approved by CEN on 21 February 2010.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 15705:2010: ESIST EN 15705:2010



EN 15705:2010 (E) 2 Contents Page Foreword .3Introduction .41Scope .52Normative references .53Terms and definitions .54Sampling and sample preparation .55Method A: Determination of CDU and IBDU .56Method B: Determination of methylen-urea oligomers (MU) .87Precision method A and method B . 138Test report . 14Annex A (informative)
Results of the inter-laboratory tests . 15Annex B (informative)
Chromatogram and calibration curves method A . 17Annex C (informative)
Chromatogram and calibration curves method B . 19Bibliography .
...

SLOVENSKI STANDARD
kSIST FprEN 15705:2009
01-november-2009
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Fertilizers - Determination of urea condensates using high-performance liquid
chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and
methylene-urea oligomers (method B)
Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-
Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff
(Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B)
Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance
(HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de
méthylene-urée (méthode B)
Ta slovenski standard je istoveten z: FprEN 15705
ICS:
65.080 Gnojila Fertilizers
kSIST FprEN 15705:2009 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST FprEN 15705:2009

---------------------- Page: 2 ----------------------
kSIST FprEN 15705:2009


EUROPEAN STANDARD
FINAL DRAFT
FprEN 15705
NORME EUROPÉENNE

EUROPÄISCHE NORM

August 2009
ICS 65.080 Will supersede CEN/TS 15705:2009
English Version
Fertilizers - Determination of urea condensates using high-
performance liquid chromatography (HPLC) -
Isobutylidenediurea and crotonylidenediurea (method A) and
methylene-urea oligomers (method B)
Engrais - Dosage des condensats d'urée par Düngemittel - Bestimmung von Harnstoffkondensaten mit
chromatographie liquide haute performance (HPLC) - Hochleistungs-Flüssigchromatographie (HPLC) -
Isobutylidène diurée et crotonylidène diurée (méthode A) et Isobutylidendiharnstoff und Crotonylidendiharnstoff
oligomères de méthylene-urée (méthode B) (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren
B)
This draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the Technical
Committee CEN/TC 260.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which
stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language
made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the
same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.



Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and
shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2009 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprEN 15705:2009: E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST FprEN 15705:2009
FprEN 15705:2009 (E)
Contents Page
Foreword .3
Introduction .4
1 Scope .5
2 Normative references .5
3 Terms and definitions .5
4 Sampling and sample preparation .5
5 Method A: Determination of CDU and IBDU .5
6 Method B: Determination of methylen-urea oligomers (MU) .8
7 Precision method A and method B .
...

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